methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

Base Information

Chemical Name:methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate
CAS No.:171513-39-6
Molecular Formula:C₃₂H₃₄N₂O₈
Molecular Weight:574.631
Hs Code.:

Synonyms:methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

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Technology Process of methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

There total 1 articles about methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 100-39-0
benzyl bromide

: 141996-73-8
methyl 5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

: 171513-39-6
methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1016/0040-4020(95)00603-6

Reference yield:

: 171513-39-6
methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

: 3(S)-benzyl-5-(2-benzyl-2,2-dimethoxycarbonyl)ethyl-2-oxo-1,2,3,6-tetrahydropyrazine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h; under 1551.4 Torr; Ambient temperature;
DOI:10.1016/0040-4020(95)00603-6

Reference yield:

: 171513-39-6
methyl 2-benzyl-5-<(N-benzyloxycarbonyl)-L-phenylalanyl>amino-2-methoxycarbonyl-4-oxopentanoate

: 141996-78-3
(4S,7R,8aR)-4,7-dibenzyl-7-methoxycarbonyl-3,6-dioxoperhydropyrrolo<1,2-a>pyrazine

: 171597-91-4
4,7-dibenzyl-7-methoxycarbonyl-3,6-dioxoperhydropyrrolo<1,2-a>pyrazine

: 4,7-dibenzyl-7-methoxycarbonyl-3,6-dioxoperhydropyrrolo<1,2-a>pyrazine

: 4,7-dibenzyl-7-methoxycarbonyl-3,6-dioxoperhydropyrrolo<1,2-a>pyrazine

Guidance literature:: With hydrogen; sodium cyanoborohydride; zinc(II) chloride; palladium on activated charcoal; Yield given. Multistep reaction. Yields of byproduct given; 1.) MeOH, RT, 40 psi, 2.) MeOH, RT;
DOI:10.1016/0040-4020(95)00603-6