2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene

Base Information

• Chemical Name: 2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene
• CAS No.: 74286-01-4
• Molecular Formula: C₃₂H₃₈N₁₁P₃
• Molecular Weight: 669.649

Synonyms:2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene

Chemical Property of 2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene

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Technology Process of 2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene

There total 1 articles about 2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ⁵,4λ⁵,6λ⁵-cyclotriphosphaza-1,3,5-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3,5-dimethyl-1H-pyrazole (67-51-6) + 2,2,4,4-tetrachloro-6,6-diphenylcyclotriphosphazatriene (2846-32-4) → 2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ5,4λ5,6λ5-cyclotriphosphaza-1,3,5-triene (74286-01-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 192h; Heating;

DOI:10.1139/v82-076

Reference yield: 95.0%

2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ5,4λ5,6λ5-cyclotriphosphaza-1,3,5-triene (74286-01-4) + copper dichloride → CuCl2(P3N3(C6H5)2(C3N2H(CH3)2)4) (164593-70-8)

Guidance literature:

In dichloromethane; according to K. R. J. Thomas, P. Tharmaraj, V. Chandrasekhar and E. R. T. Tiekink, J. Chem. Soc., Dalton Trans. 1994, 1301.; elem. anal.;

DOI:10.1016/0277-5387(94)00363-J

Reference yield: 90.0%

2,2,4,4-Tetrakis(3,5-dimethylpyrazolyl)-6,6-diphenyl-2λ5,4λ5,6λ5-cyclotriphosphaza-1,3,5-triene (74286-01-4) + copper(ll) bromide (7789-45-9) → CuBr2(P3N3(C6H5)2(C3N2H(CH3)2)4) (164593-72-0)

Guidance literature:

In dichloromethane; according to K. R. J. Thomas, P. Tharmaraj, V. Chandrasekhar and E. R. T. Tiekink, J. Chem. Soc., Dalton Trans. 1994, 1301.; elem. anal.;

DOI:10.1016/0277-5387(94)00363-J

upstream raw materials:

3,5-dimethyl-1H-pyrazole

2,2,4,4-tetrachloro-6,6-diphenylcyclotriphosphazatriene

Downstream raw materials:

CuBr₂(P₃N₃(C₆H₅)2(C₃N₂H(CH₃)2)4)

CuCl₂(P₃N₃(C₆H₅)2(C₃N₂H(CH₃)2)4)

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