1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol

Base Information

• Chemical Name: 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol
• CAS No.: 1361393-46-5
• Molecular Formula: C₄₇H₆₂N₂O₅
• Molecular Weight: 735.02
• Mol file: 1361393-46-5.mol

Synonyms:1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol

Chemical Property of 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol

There total 4 articles about 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-(nonyloxy)aniline (50262-67-4) + 2-[3-(2-formylphenoxy)-2-hydroxy propoxy]benzaldehyde (160726-74-9) → 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol (1361393-46-5)

Guidance literature:

With toluene-4-sulfonic acid; In ehanol; at 20 ℃; for 24h;

DOI:10.5012/bkcs.2012.33.5.1647

Reference yield:

4-nitrophenyl nonyl ether (86702-46-7) → 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol (1361393-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrazine hydrate

2: toluene-4-sulfonic acid / ehanol / 24 h / 20 °C

With palladium 10% on activated carbon; toluene-4-sulfonic acid; hydrazine hydrate; In ehanol;

DOI:10.5012/bkcs.2012.33.5.1647

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 1,3-Bis(2-((4-nonyloxyphenylimino)methyl)phenoxy)-propan-2-ol (1361393-46-5)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide

2: palladium 10% on activated carbon; hydrazine hydrate

3: toluene-4-sulfonic acid / ehanol / 24 h / 20 °C

With palladium 10% on activated carbon; toluene-4-sulfonic acid; hydrazine hydrate; potassium hydroxide; In ehanol;

DOI:10.5012/bkcs.2012.33.5.1647

upstream raw materials:

4-nitro-phenol

1-Bromononane

4-nitrophenyl nonyl ether

4-(nonyloxy)aniline

Refernces