t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

Base Information

Chemical Name:t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate
CAS No.:666746-68-5
Molecular Formula:C₂₅H₃₀ClNO₄
Molecular Weight:443.97
Hs Code.:

Synonyms:t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

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Chemical Property of t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

Chemical Property:

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Technology Process of t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

There total 1 articles about t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 666746-67-4
t-butyl N-t-butoxycarbonyl-4-(4-chlorobenzoyl)-2-methylcarbanilate

: 1779-49-3
Methyltriphenylphosphonium bromide

: 666746-68-5
t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.5h;

t-butyl N-t-butoxycarbonyl-4-(4-chlorobenzoyl)-2-methylcarbanilate; In tetrahydrofuran; at 20 ℃; for 1.5h;

Reference yield:

: 666746-68-5
t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

: 67-66-3,8013-54-5
chloroform

: 666746-69-6
t-butyl N-t-butoxycarbonyl-4-[2,2-dichloro-1-(4-chlorophenyl)-cyclopropyl]-2-methylcarbanilate

Guidance literature:: With sodium hydroxide; cetyltrimethylammonium chloride; In water; at 50 ℃; for 1.5h;

Reference yield:

: 666746-68-5
t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate

: 2837-90-3
sodium 2,2-dichloro-2-fluoroacetate

: 4-[2,2-difluoro-1-(4-chlorophenyl)cyclopropyl]-2-methylaniline

Guidance literature:: t-butyl N-t-butoxycarbonyl-4-[1-(4-chlorophenyl)ethenyl]-2-methylcarbanilate; sodium 2,2-dichloro-2-fluoroacetate; In 1,2-dimethoxyethane; at 170 - 180 ℃; for 1h;

With trifluoroacetic acid; at 20 ℃; for 0.25h;

With sodium hydrogencarbonate; In water; ethyl acetate;