trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Base Information

Chemical Name:trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene
CAS No.:1418200-31-3
Molecular Formula:C₂₇H₃₄N₆O₄S₂
Molecular Weight:570.737
Hs Code.:

Synonyms:trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Suppliers and Price of trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

There total 7 articles about trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1418200-30-2
trans-1-benzenesulfonyl-N*4*-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1H-pyrrolo[2,3-b]pyridine-4,5-diamine

: 78-39-7
Triethyl orthoacetate

: 1418200-31-3
trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 105 ℃; for 18h;

Reference yield:

: 1418200-25-5
trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

: 1418200-31-3
trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: Multi-step reaction with 6 steps

1: sodium acetate; acetic acid; chlorine / water

2: N-ethyl-N,N-diisopropylamine / chloroform / 3 h / 20 °C

3: dichloromethane / 2.5 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 3 h / Reflux

5: ammonium chloride; iron / water; methanol / 1.5 h / 85 °C

6: toluene-4-sulfonic acid / toluene / 18 h / 105 °C

With sodium acetate; chlorine; iron; ammonium chloride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; chloroform; water; isopropyl alcohol; toluene;

Reference yield:

: 1418200-26-6
trans-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-carbamic acid tert-butyl ester

: 1418200-31-3
trans-6-benzenesulfonyl-2-methyl-1-[4-(4-methyl-piperazine-1-sulfonylmethyl)-cyclohexyl]-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 2.5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 3 h / Reflux

3: ammonium chloride; iron / water; methanol / 1.5 h / 85 °C

4: toluene-4-sulfonic acid / toluene / 18 h / 105 °C

With iron; ammonium chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water; isopropyl alcohol; toluene;