trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

Base Information

Chemical Name:trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester
CAS No.:1418200-25-5
Molecular Formula:C₁₄H₂₅NO₃S
Molecular Weight:287.423
Hs Code.:

Synonyms:trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

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Chemical Property of trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

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Technology Process of trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

There total 3 articles about trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 947141-76-6
((1r,4r)-4-(tert-butoxycarbonylamino)cyclohexyl)methyl 4-methylbenzene-sulfonate

: 10387-40-3
potassium thioacetate

: 1418200-25-5
trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

Guidance literature:: In dimethyl sulfoxide; at 55 ℃; for 3h;

Reference yield:

: methanesulfonic acid 4-tert-butoxycarbonylamino-cyclohexylmethyl ester

: 10387-40-3
potassium thioacetate

: 1418200-25-5
trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 48h;

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1418200-25-5
trans thioacetic acid S-(4-tert-butoxycarbonylamino-cyclohexylmethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane; water / 20 °C

2: dimethyl sulfoxide / 3 h / 55 °C

With dmap; triethylamine; In dichloromethane; water; dimethyl sulfoxide;