1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

Base Information

Chemical Name:1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene
CAS No.:1616724-94-7
Molecular Formula:C₃₂H₅₂N₆O₁₀
Molecular Weight:680.799
Hs Code.:

Synonyms:1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

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Chemical Property of 1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

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Technology Process of 1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

There total 5 articles about 1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1616724-93-6
[1,3-bis(1-oxa-4,7,10-triazacyclododecan-7-yl)-methyl]benzene

: 79-08-3
bromoacetic acid

: 1616724-94-7
1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

Guidance literature:: With sodium hydroxide; In water; at 70 ℃; for 72h; pH=11;

Reference yield:

: 60147-28-6
4,7,10-tris(p-tolylsulphonyl)-1-oxa-4,7,10-triazacyclododecane

: 1616724-94-7
1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 24 h / 140 °C

2: toluene / 6 h / 60 °C / Inert atmosphere

3: acetonitrile / 6 h / 50 °C / Inert atmosphere

4: sodium hydroxide / 12 h / Reflux

5: sodium hydroxide / water / 72 h / 70 °C / pH 11

With sulfuric acid; sodium hydroxide; In water; toluene; acetonitrile;

Reference yield:

: 53835-21-5
1-oxa-4,7,10-triazacyclododecane

: 1616724-94-7
1,3-bis[4,10-bis(carboxymethyl)-1,4,10-triaza-7-oxa-cyclododec-1-ylmethyl]benzene

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 6 h / 60 °C / Inert atmosphere

2: acetonitrile / 6 h / 50 °C / Inert atmosphere

3: sodium hydroxide / 12 h / Reflux

4: sodium hydroxide / water / 72 h / 70 °C / pH 11

With sodium hydroxide; In water; toluene; acetonitrile;