Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

Base Information

Chemical Name:Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2
CAS No.:72468-44-1
Molecular Formula:C₄₅H₇₂N₁₀O₁₁S
Molecular Weight:961.193
Hs Code.:

Boc-Ile-Glu-<N(CH3)2>-Asn-Cys(Bzl)-pro-Leu-Gly-NH2

Synonyms:Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

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Chemical Property of Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

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Technology Process of Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

There total 7 articles about Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72468-46-3
N²-(tert-butyloxycarbonyl)-N⁵,N⁵-dimethylglutamine benzyl ester

: 72468-44-1
Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / H₂ / palladium oxide / propan-2-ol; H₂O / 4 h

2: 68 percent / DCC / dimethylformamide / 17 h / 0 - 4 °C

3: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

4: CF₃COOH / 0.75 h

5: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium(II) oxide; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00176a020

Reference yield:

: 72449-42-4
Boc-Gln(Me₂)-OH

: 72468-44-1
Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / DCC / dimethylformamide / 17 h / 0 - 4 °C

2: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

3: CF₃COOH / 0.75 h

4: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

With 4-methyl-morpholine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00176a020

Reference yield:

: 16748-05-3
Asn-Cys(Bzl)-Pro-Leu-Gly-NH₂

: 72468-44-1
Boc-Ile-Glu--Asn-Cys(Bzl)-pro-Leu-Gly-NH2

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

2: CF₃COOH / 0.75 h

3: N-methylmorpholine / dimethylformamide / 48 h / Ambient temperature

With 4-methyl-morpholine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00176a020