Boc-L-Tle-L-Phe-NHBu

Base Information

Chemical Name:Boc-L-Tle-L-Phe-NHBu
CAS No.:896105-74-1
Molecular Formula:C₂₄H₃₉N₃O₄
Molecular Weight:433.591
Hs Code.:

Synonyms:Boc-L-Tle-L-Phe-NHBu

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Chemical Property of Boc-L-Tle-L-Phe-NHBu

Chemical Property:

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Technology Process of Boc-L-Tle-L-Phe-NHBu

There total 3 articles about Boc-L-Tle-L-Phe-NHBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62965-35-9
N-tert-butyloxycarbonyl-L-tert-leucine

: 1236254-97-9
L-Phe-NHBu*HCl

: 896105-74-1
Boc-L-Tle-L-Phe-NHBu

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 22 ℃; for 4h;
DOI:10.1021/ja061166o

Reference yield:

: 112670-44-7
1-butylcarbamoyl-2-phenyl-ethyl-carbamic acid tert butyl ester

: 896105-74-1
Boc-L-Tle-L-Phe-NHBu

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / aq. HCl / dioxane / 0.5 h / 22 °C

2: HOBt*H₂O; EDC*HCl; Et₃N / CH₂Cl₂ / 4 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja061166o

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 896105-74-1
Boc-L-Tle-L-Phe-NHBu

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / HOBt*H₂O; EDC*HCl / CH₂Cl₂ / 4 h / 22 °C

2: 88 percent / aq. HCl / dioxane / 0.5 h / 22 °C

3: HOBt*H₂O; EDC*HCl; Et₃N / CH₂Cl₂ / 4 h / 22 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ja061166o