(1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate

Base Information

• Chemical Name: (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate
• CAS No.: 1236266-09-3
• Molecular Formula: C₂HF₃O₂*C₁₇H₂₃N₅O₃S₂
• Molecular Weight: 523.557

Synonyms:(1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate

Chemical Property of (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate

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Technology Process of (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate

There total 1 articles about (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl ((1r,4r)-4-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenylcarbamoyl)cyclohexyl)methylcarbamate + trifluoroacetic acid (76-05-1) → (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate (1236266-09-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

Reference yield:

4,6-dichloro-N-(2,3-dimethylbenzyl)-1,3,5-triazin-2-amine (1236266-12-8) + (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate (1236266-09-3) → (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236266-15-1)

Guidance literature:

With sodium hydroxide; In water; acetonitrile; at 20 ℃; pH=9 - 10;

Reference yield:

4,6-dichloro-N-(3-chloro-2-methylbenzyl)-1,3,5-triazin-2-amine (1236266-14-0) + (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate (1236266-09-3) → (1r,4r)-4-((4-chloro-6-(3-chloro-2-methylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236266-16-2)

Guidance literature:

With sodium hydroxide; In water; acetonitrile; at 20 ℃; pH=9 - 10;

upstream raw materials:

trifluoroacetic acid

Downstream raw materials:

(1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

(1r,4r)-4-((4-chloro-6-(3-chloro-2-methylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

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