(1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

Base Information

• Chemical Name: (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide
• CAS No.: 1236266-15-1
• Molecular Formula: C₂₉H₃₄ClN₉O₃S₂
• Molecular Weight: 656.232

Synonyms:(1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

Chemical Property of (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

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Technology Process of (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

There total 1 articles about (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,6-dichloro-N-(2,3-dimethylbenzyl)-1,3,5-triazin-2-amine (1236266-12-8) + (1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate (1236266-09-3) → (1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236266-15-1)

Guidance literature:

With sodium hydroxide; In water; acetonitrile; at 20 ℃; pH=9 - 10;

Reference yield:

(1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236266-15-1) + benzylamine (100-46-9) → (1r,4r)-4-((4-(benzylamino)-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236265-39-6)

Guidance literature:

In water; acetonitrile; at 80 ℃;

Reference yield:

(1r,4r)-4-((4-chloro-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236266-15-1) + methylamine (74-89-5) → (1r,4r)-4-((4-(2,3-dimethylbenzylamino)-6-(methylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide (1236265-41-0)

Guidance literature:

In water; acetonitrile; at 80 ℃;

upstream raw materials:

4,6-dichloro-N-(2,3-dimethylbenzyl)-1,3,5-triazin-2-amine

(1r,4r)-4-(aminomethyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide trifluoroacetate

Downstream raw materials:

(1r,4r)-4-((4-(benzylamino)-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

(1r,4r)-4-((4-(2,3-dimethylbenzylamino)-6-(methylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

(1r,4r)-4-((4-(2-(dimethylamino)ethylamino)-6-(2,3-dimethylbenzylamino)-1,3,5-triazin-2-ylamino)methyl)-N-(4-(N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfamoyl)phenyl)cyclohexanecarboxamide

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