benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

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Chemical Name:benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester
CAS No.:1187618-32-1
Molecular Formula:C₂₂H₃₂O₇
Molecular Weight:408.492
Hs Code.:

Synonyms:benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

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Technology Process of benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

There total 1 articles about benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1187618-31-0
benzoic acid (S)-3-(tert-butyl-dimethyl-silanyloxymethyl)-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

: 1187618-32-1
benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

Guidance literature:: benzoic acid (S)-3-(tert-butyl-dimethyl-silanyloxymethyl)-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

With ammonium chloride; In tetrahydrofuran; water; Saturated solution;
DOI:10.1016/j.tet.2009.04.021

Reference yield: 82.0%

: 1187618-32-1
benzoic acid (S)-3-hydroxymethyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enyl ester

: 1187618-33-2
benzoic acid (1S,5S)-3-formyl-1,5-bis-methoxymethoxy-2,2,4-trimethyl-cyclohex-3-enylmethyl ester

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2009.04.021