2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

Base Information

Chemical Name:2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene
CAS No.:118722-59-1
Molecular Formula:C₁₂H₂₅NOSi
Molecular Weight:227.422
Hs Code.:

Synonyms:2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

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Chemical Property of 2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

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Technology Process of 2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

There total 2 articles about 2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 32367-49-0
allyl(bromomethyl)dimethylsilane

: 63126-47-6
(2S)-2-(methoxymethyl)-1-pyrrolidine

: 118722-59-1
2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

Guidance literature:: at 80 ℃; for 20h;
DOI:10.1016/S0040-4039(00)99397-3

Reference yield: 74.0%

: 33558-75-7
allyl(chloromethyl)dimethylsilane

: 63126-47-6
(2S)-2-(methoxymethyl)-1-pyrrolidine

: 118722-59-1
2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

Guidance literature:: at 80 ℃; for 24h;
DOI:10.1021/jo00263a012

Reference yield:

: 118722-59-1
2,2-dimethyl-1-<1-<(S)-2-(methoxymethyl)pyrrolidinyl>>-2-sila-4-pentene

: 100-52-7
benzaldehyde

: (Z)-4-[((S)-2-Methoxymethyl-pyrrolidin-1-ylmethyl)-dimethyl-silanyl]-1-phenyl-but-3-en-1-ol

: (E)-4-[((S)-2-Methoxymethyl-pyrrolidin-1-ylmethyl)-dimethyl-silanyl]-1-phenyl-but-3-en-1-ol

Guidance literature:: With n-butyllithium; potassium tert-butylate; Yield given; Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) Et₂O, hexane, from -70 deg C to RT, 4 h, 2.) Et₂O, hexane, a) -78 deg C, 6 h, b) RT, 12 h;
DOI:10.1039/a802886i