tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

Base Information

Chemical Name:tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate
CAS No.:105259-81-2
Molecular Formula:C₃₉H₅₅N₃O₇
Molecular Weight:677.882
Hs Code.:

tert-butyl N-<N-<(1R)-5-(1-benzyloxycarbonyl-4-piperidyl)-1-ethoxycarbonylpentyl>-L-alanyl>-N-(2-indanyl)glycinate

Synonyms:tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

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Chemical Property of tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

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Technology Process of tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

There total 4 articles about tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 99198-61-5
ethyl 6-(1-benzyloxycarbonyl-4-piperidyl)-2-oxohexanoate

: 108428-37-1
N-(L-alanyl)-N-(2-indanyl)glycine tert-butyl ester oxalate

: 105259-81-2
tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

: 105259-82-3
tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

Guidance literature:: With 3 A molecular sieve; sodium acetate; sodium cyanoborohydride; acetic acid; In ethanol;
DOI:10.1248/cpb.42.580

Reference yield:

: 99198-61-5
ethyl 6-(1-benzyloxycarbonyl-4-piperidyl)-2-oxohexanoate

: 108428-37-1
N-(L-alanyl)-N-(2-indanyl)glycine tert-butyl ester oxalate

: 105259-81-2
tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

Guidance literature:: With sodium acetate; sodium cyanoborohydride; acetic acid; silica gel; In ethanol; water;

Reference yield:

: 105259-96-9
tert-butyl-N-<(1R)-5-(1-benzyloxycarbonyl-4-piperidyl)-1-ethoxycarbonylpentyl>-L-alaninate

: 105259-81-2
tert-butyl N--L-alanyl>-N-(2-indanyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 5 N HCl / ethyl acetate / 4 h

2: 1.) diethyl phosphorocyanidate (DEPC), 2.) Et₃N / 1.) DMF, 30 min, 2.) DMF, a) 0 deg C, 30 min, b) RT, 30 min

With hydrogenchloride; diethyl cyanophosphonate; triethylamine; In ethyl acetate;
DOI:10.1248/cpb.42.580