C₁₂H₁₄O₃

Base Information

Chemical Name:C₁₂H₁₄O₃
CAS No.:1609109-71-8
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:

C<sub>12</sub>H<sub>14</sub>O<sub>3</sub>

Synonyms:C₁₂H₁₄O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₄O₃

Chemical Property:

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Technology Process of C₁₂H₁₄O₃

There total 1 articles about C₁₂H₁₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 201230-82-2
carbon monoxide

: 98453-57-7
4-(4-bromophenyl)butanoic acid methyl ester

: 1609109-71-8
C₁₂H₁₄O₃

Guidance literature:: With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/j.bmcl.2014.03.090

Reference yield: 99.0%

: 600-00-0
ethyl 2-bromoisobutyrate

: 1609109-71-8
C₁₂H₁₄O₃

: 1609109-72-9
C₁₈H₂₆O₅

Guidance literature:: With iodine; zinc; at 20 ℃; Sonication;
DOI:10.1016/j.bmcl.2014.03.090

Reference yield:

: 1609109-71-8
C₁₂H₁₄O₃

: 1609109-68-3
C₃₅H₄₄N₄O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: zinc; iodine / 20 °C / Sonication

2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

3: potassium trimethylsilonate / tetrahydrofuran / 20 °C

4: O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

5: camphor-10-sulfonic acid / ethyl acetate / 80 °C

6: lithium hydroxide; water / tetrahydrofuran; methanol / 20 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With triethylsilane; dmap; boron trifluoride diethyl etherate; potassium trimethylsilonate; water; iodine; camphor-10-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N,N-tetramethyluroniumhexafluorophosphate; lithium hydroxide; zinc; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 1: |Reformatsky Reaction;
DOI:10.1016/j.bmcl.2014.03.090