(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

Base Information

Chemical Name:(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose
CAS No.:266306-54-1
Molecular Formula:C₂₄H₃₁NO₅Si
Molecular Weight:441.599
Hs Code.:

Synonyms:(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

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Technology Process of (E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

There total 1 articles about (E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75783-45-8
(3aR,5R,6aS)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]-2,2-dimethyltetrahydro-2H-furo[2,3-d][1,3]dioxol-6-one

: 266306-54-1
(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol;
DOI:10.1039/a806326e

Reference yield: 91.0%

: 266306-54-1
(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

: 217438-62-5
5-O-(tert-butyldiphenylsilyl)-3-chloro-3-deoxy-1,2-O-isopropylidene-3-C-nitroso-α-D-xylofuranose

Guidance literature:: With tert-butylhypochlorite; In dichloromethane; at -10 ℃; for 0.25h;

Reference yield:

: 266306-54-1
(E/Z)-5-O-(tert-Butyldiphenylsilyl)-3-deoxy-3-hydroxyimino-1,2-O-isopropylidene-α-D-erythro-pentofuranose

: 217438-64-7
C₂₉H₃₆ClNO₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOCl / CH₂Cl₂

2: 93 percent / CHCl₃ / Ambient temperature

With tert-butylhypochlorite; In dichloromethane; chloroform;
DOI:10.1039/a806326e