C₃₃H₃₇N₃O₄

Base Information

Chemical Name:C₃₃H₃₇N₃O₄
CAS No.:1384107-27-0
Molecular Formula:C₃₃H₃₇N₃O₄
Molecular Weight:539.674
Hs Code.:

C<sub>33</sub>H<sub>37</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₃₃H₃₇N₃O₄

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Chemical Property of C₃₃H₃₇N₃O₄

Chemical Property:

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Technology Process of C₃₃H₃₇N₃O₄

There total 8 articles about C₃₃H₃₇N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1384107-26-9
C₃₉H₄₃N₃O₄Se

: 1384107-27-0
C₃₃H₃₇N₃O₄

: 1384107-31-6
C₃₃H₃₇N₃O₄

Guidance literature:: With pyridine; 3-chloro-benzenecarboperoxoic acid; In hexane; dichloromethane; at -30 - 20 ℃;
DOI:10.1021/ol301331t

Reference yield:

: 100-39-0
benzyl bromide

: 1384107-27-0
C₃₃H₃₇N₃O₄

: 1384107-31-6
C₃₃H₃₇N₃O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C / Cooling with ice

2.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 0 °C

2.2: 0 °C

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 24 h / 0 °C

4.1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C

5.1: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere

6.1: sodium tetrahydroborate / ethanol / 2 h / 25 °C

7.1: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C

With pyridine; 2,6-dimethylpyridine; imidazole-1-sulfonyl azide hydrochloride; sodium tetrahydroborate; copper(ll) sulfate pentahydrate; t-butyldimethylsiyl triflate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In methanol; ethanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1021/ol301331t

Reference yield:

: 844856-96-8
[2-hydroxy-2-(8-hydroxy-1,4-dioxaspiro[4.5]dec-7-yl)-1-(4-methoxybenzyl)ethyl]carbamic acid tert-butyl ester

: 1384107-27-0
C₃₃H₃₇N₃O₄

: 1384107-31-6
C₃₃H₃₇N₃O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C / Cooling with ice

2.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 0 °C

2.2: 0 °C

3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 24 h / 0 °C

4.1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C

5.1: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere

6.1: sodium tetrahydroborate / ethanol / 2 h / 25 °C

7.1: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C

With pyridine; 2,6-dimethylpyridine; imidazole-1-sulfonyl azide hydrochloride; sodium tetrahydroborate; copper(ll) sulfate pentahydrate; t-butyldimethylsiyl triflate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In methanol; ethanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1021/ol301331t