p-methy lphenylfluorosulfate

Base Information

• Chemical Name: p-methy lphenylfluorosulfate
• CAS No.: 660-34-4
• Molecular Formula: C₇H₇FO₃S
• Molecular Weight: 190.195
• Mol file: 660-34-4.mol

Synonyms:p-methy lphenylfluorosulfate

Chemical Property of p-methy lphenylfluorosulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-methy lphenylfluorosulfate

There total 2 articles about p-methy lphenylfluorosulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p-cresol (106-44-5) → p-methy lphenylfluorosulfate (660-34-4)

Guidance literature:

With fluorosulfonyl fluoride; triethylamine; In 1,4-dioxane; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1021/acs.orglett.9b00836

Reference yield:

→ p-methy lphenylfluorosulfate (660-34-4)

Guidance literature:

4-CH3-C6H4ONa, SO2F2;

Reference yield: 97.0%

p-methy lphenylfluorosulfate (660-34-4) + 1-Naphthylboronic acid (13922-41-3) → 1-(4-methylphenyl)naphthalene (27331-34-6)

Guidance literature:

With palladium diacetate; triethylamine; triphenylphosphine; In 1,4-dioxane; water; at 60 ℃; for 12h;

DOI:10.1021/acscatal.5b01021

upstream raw materials:

p-cresol

Downstream raw materials:

4-(4-tolyl)anisole

1-(4-methylphenyl)naphthalene

4-(p-tolyl)pyridine

4-Methylbiphenyl