4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

Base Information

Chemical Name:4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline
CAS No.:1402151-93-2
Molecular Formula:C₂₈H₃₉NSiSn
Molecular Weight:536.42
Hs Code.:

Synonyms:4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

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Technology Process of 4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

There total 1 articles about 4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1372107-28-2
4-bromo-N-(4-(t-butyl)phenyl)-N-(4-(trimethylsilyl)phenyl)aniline

: 1066-45-1
trimethyltin(IV)chloride

: 1402151-93-2
4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

Guidance literature:: 4-bromo-N-(4-(t-butyl)phenyl)-N-(4-(trimethylsilyl)phenyl)aniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;

trimethyltin(IV)chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201502268

Reference yield: 66.0%

: 1402151-93-2
4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

: 1402151-94-3
4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(dibromoboryl)phenyl)aniline

: 2,4,6-triisopropylphenyl copper(I)

: 1402151-90-9
C₆₅H₈₃BN₂Si₂

Guidance literature:: In not given; two steps; boron compd. treated with Sn compd., treatment with TipCu;
DOI:10.1002/anie.201203788

Reference yield: 62.0%

: 1402151-93-2
4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline

: t-Butyl-N,N-bis(4-dibromoborylphenyl)aniline

: 2,4,6-triisopropylphenyl copper(I)

: C₁₀₂H₁₂₇B₂N₃Si₂

Guidance literature:: 4-(t-butyl)-N-(4-(trimethylsilyl)phenyl)-N-(4-(trimethylstannyl)phenyl)aniline; t-Butyl-N,N-bis(4-dibromoborylphenyl)aniline; In dichloromethane;

2,4,6-triisopropylphenyl copper(I); In toluene; at 120 ℃; for 48h; Inert atmosphere;
DOI:10.1002/chem.201502268