4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

Base Information

Chemical Name:4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine
CAS No.:1569033-04-0
Molecular Formula:C₁₆H₈F₉N₃O
Molecular Weight:429.245
Hs Code.:

Synonyms:4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

Chemical Property:

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Technology Process of 4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

There total 2 articles about 4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 110-91-8,99108-56-2
morpholine

: 42289-22-5
4-chloro-2,3,4,5,6-pentafluorocyclohexa-2,5-dienone

: aluminum trichloride-pentafluorophenylhydrazine complex

: 771-60-8
2,3,4,5,6-pentafluoroaniline

: 1569033-04-0
4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

Guidance literature:: morpholine; 4-chloro-2,3,4,5,6-pentafluorocyclohexa-2,5-dienone; In diethyl ether; for 0.5h;

aluminum trichloride-pentafluorophenylhydrazine complex; In diethyl ether; at 0 - 20 ℃; for 20h;
DOI:10.1134/S1070428014010060

Reference yield:

: 828-73-9
pentafluorophenyl hydrazine

: 1569033-04-0
4-{2,4,5,6-tetrafluoro-3-[(pentafluorophenyl)diazenyl]phenyl}morpholine

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / 0 °C

2.1: diethyl ether / 0.5 h

2.2: 20 h / 0 - 20 °C

In diethyl ether;
DOI:10.1134/S1070428014010060