acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

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Chemical Name:acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester
CAS No.:877082-51-4
Molecular Formula:C₃₅H₅₅NO₇S₄
Molecular Weight:730.088
Hs Code.:

Synonyms:acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

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Chemical Property of acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

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Technology Process of acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

There total 5 articles about acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 877082-49-0
(1-vinyl-hexyl)carbamic acid benzyl ester

: 877082-50-3
acetic acid 2,6-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-hexyl ester

: 877082-51-4
acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

Guidance literature:: With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;
DOI:10.1039/b514509k

Reference yield:

: 877082-48-9
(1-benzenesulfonyl-hexyl)carbamic acid benzyl ester

: 877082-51-4
acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / tetrahydrofuran / 1 h / 0 °C

2: 65 percent / dilauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1039/b514509k

Reference yield:

: 2442-10-6
oct-1-en-3-yl acetate

: 877082-51-4
acetic acid 9-benzyloxycarbonylamino-2,8-bis(ethoxythiocarbonylsulfanyl)-5-oxo-1-pentyl-tetradecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dilauroyl peroxide / 1,2-dichloro-ethane / 1 h / Heating

1.2: 98 percent / acetone / 1 h / 20 °C

2.1: 65 percent / dilauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane;
DOI:10.1039/b514509k