C₆H₅C(OH)CHC(CF₃)NC₆H₅

Base Information

Chemical Name:C₆H₅C(OH)CHC(CF₃)NC₆H₅
CAS No.:1020853-33-1
Molecular Formula:C₁₆H₁₂F₃NO
Molecular Weight:291.273
Hs Code.:

C<sub>6</sub>H<sub>5</sub>C(OH)CHC(CF<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>

Synonyms:C₆H₅C(OH)CHC(CF₃)NC₆H₅

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Chemical Property of C₆H₅C(OH)CHC(CF₃)NC₆H₅

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Technology Process of C₆H₅C(OH)CHC(CF₃)NC₆H₅

There total 1 articles about C₆H₅C(OH)CHC(CF₃)NC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66929-54-2
1,1,1-trifluoro-4-hydroxy-4-phenyl-but-3-en-2-one

: 62-53-3
aniline

: 1020853-33-1
C₆H₅C(OH)CHC(CF₃)NC₆H₅

Guidance literature:: In toluene; Acidic conditions;
DOI:10.1039/c0dt01225d

Reference yield: 81.1%

: 109-72-8,29786-93-4
n-butyllithium

: 1020853-33-1
C₆H₅C(OH)CHC(CF₃)NC₆H₅

: 7550-45-0
titanium tetrachloride

: [TiCl₂(CO(C₆H₅)CHC(CF₃)N(C₆H₅))2]

Guidance literature:: In diethyl ether; hexane; to soln. of ligand in Et2O at -78°C was added BuLi (in hexane), mixt. was warmed to room temp., stirred for 2.5 h, then added to TiCl4 inEt2O at -78°C over 30 min with stirring, mixt. was warmed to roo m temp., stirred for 16 h; mixt. was evapd., CH2Cl2 was added, mixt. stirred for 10 min, filtered, filtrate was evapd., Et2O and hexane were added to residue, mixt. stirred for 10 min, ppt. was filtered off; elem. anal.;
DOI:10.1021/om030396y

Reference yield: 68.0%

: 10170-68-0,16997-54-9
trichlorotris(tetrahydrofuran)chromium(III)

: 1020853-33-1
C₆H₅C(OH)CHC(CF₃)NC₆H₅

: lithium cyclopentadienide

: Cp[(C₆H₅)NC(CF₃)C(H)C(Ph)O]CrCl

Guidance literature:: trichlorotris(tetrahydrofuran)chromium(III); lithium cyclopentadienide; In tetrahydrofuran; at 0 - 20 ℃;

C₆H₅C(OH)CHC(CF₃)NC₆H₅; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.molcata.2014.07.006