N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Base Information

Chemical Name:N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide
CAS No.:1430973-40-2
Molecular Formula:C₁₆H₁₅Br₂NO₂
Molecular Weight:413.109
Hs Code.:

Synonyms:N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Suppliers and Price of N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

There total 2 articles about N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 618-58-6
3,5-dibromobenzoic acid

: 3182-95-4
L-Phenylalaninol

: 1430973-40-2
N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Guidance literature:: 3,5-dibromobenzoic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

L-Phenylalaninol; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/pola.26499

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1430973-40-2
N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate; sulfuric acid / tetrahydrofuran; diethyl ether / 20 °C

2.1: 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium tetrahydroborate; 1-hydroxy-pyrrolidine-2,5-dione; sulfuric acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether;
DOI:10.1002/pola.26499

Reference yield: 54.0%

: 1430973-40-2
N-((S)-1-benzyl-2-hydroxyethyl)-3,5-dibromobenzamide

: 1430973-43-5
(S)-4-benzyl-2-(3,5-dibromophenyl)oxazoline

Guidance literature:: With dmap; triethylamine; p-toluenesulfonyl chloride; In 1,2-dichloro-ethane; at 0 ℃; for 12h; Reflux;
DOI:10.1002/pola.26499