9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene

Base Information

• Chemical Name: 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene
• CAS No.: 126431-49-0
• Molecular Formula: C₂₁H₁₃N₅O₈
• Molecular Weight: 463.363
• Mol file: 126431-49-0.mol

Synonyms:9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene

Chemical Property of 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene

There total 2 articles about 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,4,5,7-tetranitro-9H-fluorene (29210-71-7) + N-methyl-N-phenylformamide (93-61-8) → 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene (126431-49-0)

Guidance literature:

With acetic anhydride; at 95 ℃; for 1h;

Reference yield: 76.0%

9-hydroxymethylene-2,4,5,7-tetranitrofluorene (126431-57-0) + N-methylaniline (100-61-8) → 9-(N-methyl-N-phenylaminomethylene)-2,4,5,7-tetranitrofluorene (126431-49-0)

Guidance literature:

In acetonitrile; for 1h;

upstream raw materials:

2,4,5,7-tetranitro-9H-fluorene

N-methyl-N-phenylformamide

9-hydroxymethylene-2,4,5,7-tetranitrofluorene

N-methylaniline

Refernces