(S)-1-acetoxy-1-phenyl-2-chloroethane

Base Information

Chemical Name:(S)-1-acetoxy-1-phenyl-2-chloroethane
CAS No.:103665-43-6
Molecular Formula:C₁₀H₁₁ClO₂
Molecular Weight:198.649
Hs Code.:

Synonyms:(S)-1-acetoxy-1-phenyl-2-chloroethane

Suppliers and Price of (S)-1-acetoxy-1-phenyl-2-chloroethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-1-acetoxy-1-phenyl-2-chloroethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-1-acetoxy-1-phenyl-2-chloroethane

There total 23 articles about (S)-1-acetoxy-1-phenyl-2-chloroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-22-5
Isopropenyl acetate

: 1674-30-2
1-phenyl-2-chloroethanol

: 103665-43-6
(S)-1-acetoxy-1-phenyl-2-chloroethane

Guidance literature:: With dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; sodium carbonate; In tetrahydrofuran; toluene; at 20 ℃; for 24h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ol801749z

Reference yield: 48.0%

: 108-22-5
Isopropenyl acetate

: 532-27-4,108321-66-0,164322-25-2
1-chloroacetophenone

: 56751-12-3
2-chloro-1-phenylethanol

: 103665-43-6
(S)-1-acetoxy-1-phenyl-2-chloroethane

Guidance literature:: 1-chloroacetophenone; With aluminum oxide; sodium tetrahydroborate; In hexane; at 40 ℃; for 3h;

Isopropenyl acetate; With Lipase 'Amano' PS-C II; In hexane; at 25 ℃; for 10h;
DOI:10.1016/S0957-4166(02)00170-2

Reference yield: 43.0%

: 108-05-4,9003-20-7
vinyl acetate

: 1674-30-2
1-phenyl-2-chloroethanol

: 70111-05-6
(S)-2-chloro-1-phenylethanol

: 56751-12-3
2-chloro-1-phenylethanol

: 103665-43-6
(S)-1-acetoxy-1-phenyl-2-chloroethane

Guidance literature:: 1-phenyl-2-chloroethanol; With Burkholderia cepacia lipase; In diethyl ether; at 30 ℃; for 0.5h; Enzymatic reaction;

vinyl acetate; In diethyl ether; at 30 ℃; for 2.5h; optical yield given as %ee; enantioselective reaction; Enzymatic reaction;
DOI:10.1016/j.tet.2009.09.058