Technology Process of 11-Hexadecynyl acetate
There total 10 articles about 11-Hexadecynyl acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iron(III) chloride;
In
dichloromethane;
at -30 ℃;
for 3h;
DOI:10.1055/s-2000-6258
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) Na2SO3, NaHCO3 / 1.) H2O, 10 h, 2.) 1 h
2: Et3N / CH2Cl2 / 1 h / Ambient temperature
3: 1.) Mg / 1.) Et2O, 2.) reflux, 1 h
4: (AcO)2Cu / acetic acid; H2O / 0.67 h / Heating
5: 85percent hydrazine hydrate / butan-1-ol / Heating
6: O2, CuCl / pyridine
7: acetic acid / 10 h / 50 °C
With
oxygen; copper diacetate; sodium hydrogencarbonate; hydrazine hydrate; magnesium; triethylamine; copper(l) chloride; sodium sulfite;
In
pyridine; dichloromethane; water; acetic acid; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Et3N / CH2Cl2 / 1 h / Ambient temperature
2: 1.) Mg / 1.) Et2O, 2.) reflux, 1 h
3: (AcO)2Cu / acetic acid; H2O / 0.67 h / Heating
4: 85percent hydrazine hydrate / butan-1-ol / Heating
5: O2, CuCl / pyridine
6: acetic acid / 10 h / 50 °C
With
oxygen; copper diacetate; hydrazine hydrate; magnesium; triethylamine; copper(l) chloride;
In
pyridine; dichloromethane; water; acetic acid; butan-1-ol;
