tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Base Information

Chemical Name:tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate
CAS No.:848034-55-9
Molecular Formula:C₃₉H₃₆O₁₁
Molecular Weight:680.708
Hs Code.:

Synonyms:tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Suppliers and Price of tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

There total 2 articles about tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 848034-51-5
(2R,3R,4S,5R,6R)-3,4,5-tris(benzoyloxy)-6-((benzoyloxy)methyl)tetrahydro-2H-pyran-2-carboxylic acid

: 540-88-5
acetic acid tert-butyl ester

: 848034-55-9
tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: With perchloric acid; In water; at 20 ℃; for 72h;
DOI:10.1016/j.tetasy.2004.11.064

Reference yield:

: 286369-06-0
2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonamide

: 848034-55-9
tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / nitrogen(IV) oxide / CH₂Cl₂ / 20 °C

2: 73 percent / perchloric acid / H₂O / 72 h / 20 °C

With perchloric acid; Nitrogen dioxide; In dichloromethane; water;
DOI:10.1016/j.tetasy.2004.11.064

Reference yield:

: 848034-55-9
tert-butyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

: tert-butyl 2-azido-3,4,5,7-tetra-O-benzoyl-2-deoxy-β-D-gluco-hept-2-ulopyranosonate

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide / Heating

2: 0.05 g / sodium azide / dimethylsulfoxide / 20 °C

With N-Bromosuccinimide; sodium azide; In dimethyl sulfoxide;
DOI:10.1016/j.tetasy.2004.11.064