{K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

Base Information

Chemical Name:{K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}
CAS No.:85422-35-1
Molecular Formula:C₁₂H₂₄KO₆*C₃₈H₄₁B₉P₂Rh
Molecular Weight:1063.31
Hs Code.:

{K(C<sub>2</sub>H<sub>4</sub>O)6}<sup>(1+)</sup>*{(P(C<sub>6</sub>H<sub>5</sub>)3)2RhC<sub>2</sub>B<sub>9</sub>H<sub>11</sub>}<sup>(1-)</sup>={K(C<sub>2</sub>H<sub>4</sub>O)6}{(P(C<sub>6</sub>H<sub>5</sub>)3)2RhC<sub>2</sub>B<sub>9</sub>H<sub>11</sub>}

Synonyms:{K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

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Chemical Property of {K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

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Technology Process of {K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

There total 1 articles about {K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 17455-13-9
18-crown-6 ether

: 53687-46-0
closo-3,3-(PPh₃)2-3-H-3,1,2-RhC₂B₉H₁₁

: 85422-35-1
{K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

Guidance literature:: With KOH; In tetrahydrofuran; ethanol; under N2, borane is added to a soln. of 18-crown-6 and KOH in THF/EtOH,2 h; soln. is concd., EtOH is added, filtn., crystals washed;

Reference yield: 55.0%

: 85422-35-1
{K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)2RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)2RhC₂B₉H₁₁}

: 100-39-0
benzyl bromide

: {K(C₂H₄O)6}⁽¹⁺⁾*{(P(C₆H₅)3)(C₆H₅CH₂)(Br)RhC₂B₉H₁₁}^(1-)={K(C₂H₄O)6}{(P(C₆H₅)3)(C₆H₅CH₂)(Br)RhC₂B₉H₁₁}

Guidance literature:: In benzene; addn. of benzyl bromide to suspension of complex, stirred for 1.5 h under N2; decanted, washed repeatedly (diethyl ether), dried (vac.), recrystd. once (THF/heptane) and twice (CH2Cl2/heptane); elem. anal.;