methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

Base Information

Chemical Name:methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside
CAS No.:1332832-41-3
Molecular Formula:C₂₇H₂₆F₄O₇S
Molecular Weight:570.559
Hs Code.:

Synonyms:methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

Suppliers and Price of methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

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Technology Process of methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

There total 1 articles about methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 87586-11-6
Methyl 4-Deoxy-4-fluoro-6-O-trityl-α-D-talopyranoside

: 1332832-42-4
methyl 2,4-dideoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-threo-hex-2-enopyranoside

: 1332832-41-3
methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 - 23 ℃; for 1h;
DOI:10.1016/j.jfluchem.2011.05.017

Reference yield: 68.0%

: 1332832-41-3
methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

: 127-09-3
sodium acetate

: 1332832-43-5
methyl 3-O-acetyl-4-deoxy-4-fluoro-6-O-trityl-α-D-idopyranoside

Guidance literature:: In N,N-dimethyl-formamide; at 40 ℃; for 6h;
DOI:10.1016/j.jfluchem.2011.05.017

Reference yield:

: 1332832-41-3
methyl 4-deoxy-4-fluoro-3-O-trifluoromethanesulfonyl-6-O-trityl-α-D-talopyranoside

: 1332832-39-9
methyl 4-deoxy-4-fluoro-6-O-trityl-α-D-idopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 6 h / 40 °C

2.1: sodium methylate / methanol / 3 h / 23 °C

2.2: Dowex gel 50W-X₈ (H+ form)

With sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2011.05.017