methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

Base Information

Chemical Name:methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside
CAS No.:115350-44-2
Molecular Formula:C₂₅H₃₀NO₁₁P
Molecular Weight:551.487
Hs Code.:

Synonyms:methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

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Technology Process of methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

There total 3 articles about methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 84868-33-7
methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-α-D-glucopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 115350-44-2
methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

Guidance literature:: With pyridine; dmap; In benzene; at 20 ℃; for 1h;
DOI:10.1007/BF00958357

Reference yield:

: 84868-33-7
methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-α-D-glucopyranoside

: 115350-44-2
methyl 2-acetamido-3,4-di-O-acetyl-2-desoxy-6-O-diphenylphosphoryl-α-D-glucoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / butyllithium / tetrahydrofuran; pentane / -70 °C

2: tetrahydrofuran; pentane / 0.05 h

With n-butyllithium; In tetrahydrofuran; pentane;
DOI:10.1007/BF00958357