C₅₆H₈₂O₇S₂Si₂

Base Information

Chemical Name:C₅₆H₈₂O₇S₂Si₂
CAS No.:344315-40-8
Molecular Formula:C₅₆H₈₂O₇S₂Si₂
Molecular Weight:987.566
Hs Code.:

C<sub>56</sub>H<sub>82</sub>O<sub>7</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₅₆H₈₂O₇S₂Si₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₆H₈₂O₇S₂Si₂

Chemical Property:

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Technology Process of C₅₆H₈₂O₇S₂Si₂

There total 21 articles about C₅₆H₈₂O₇S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 82192-59-4
1,3-bis(triisopropylsilyl)prop-1-yne

: 344315-39-5
C₄₄H₆₀O₈S₂Si

: 344315-40-8
C₅₆H₈₂O₇S₂Si₂

Guidance literature:: With n-butyllithium;
DOI:10.1016/S0040-4039(01)00286-6

Reference yield:

: (2S,3S,4R,4aR,6R,7S,8aR)-2-Allyl-3,4-bis-benzyloxy-6-(3,3-dibromo-allyl)-7-(1-ethoxy-ethoxy)-octahydro-pyrano[3,2-b]pyran

: 344315-40-8
C₅₆H₈₂O₇S₂Si₂

Guidance literature:: Multi-step reaction with 21 steps

1.1: n-BuLi / tetrahydrofuran

2.1: Amberlyst-15E / methanol

3.1: Co₂(CO)8; BF₃*OEt₂ / CH₂Cl₂

3.2: propargyl alcohol / 1,2-dichloro-ethane / 60 °C

4.1: Jones' reagent / acetone

4.2: 88 percent / PdCl₂; CuCl / dimethylformamide; H₂O

5.1: 86 percent / I(collidine)2PF₆- / CH₂Cl₂

6.1: 90 percent / BF₃*OEt₂ / CH₂Cl₂

7.1: DIBAL-H / CH₂Cl₂

8.1: DBU / tetrahydrofuran

9.1: 81 percent / K₂CO₃ / methanol

10.1: 90 percent / BF₃*OEt₂ / CH₂Cl₂

11.1: p-nitro benzoic acid; DEAD; PPh₃ / toluene

11.2: 94 percent / K₂CO₃ / methanol

12.1: PPTS / CH₂Cl₂

13.1: n-BuLi / tetrahydrofuran

14.1: Amberlyst-15E / methanol

15.1: Jones' reagent / acetone

16.1: I(collidine)2PF₆ / CH₂Cl₂

17.1: BF₃*OEt₂ / CH₂Cl₂

18.1: DIBAL-H / CH₂Cl₂

19.1: DBU / tetrahydrofuran

20.1: 69 percent / n-BuLi

With n-butyllithium; jones' reagent; dicobalt octacarbonyl; Amberlyst-15E; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 4.1: Wacker oxidation / 11.1: modified Mitsunobu inversion;
DOI:10.1016/S0040-4039(01)00286-6

Reference yield:

: 344315-43-1
(2S,3S,4R,4aR,5aR,8S,9R,10aS,11aR)-3,4-Bis-benzyloxy-2-(2-methyl-[1,3]dithian-2-ylmethyl)-9-prop-2-ynyl-2,3,4,4a,5a,8,9,10a,11,11a-decahydro-1,5,10-trioxa-cyclohepta[b]naphthalen-8-ol

: 344315-40-8
C₅₆H₈₂O₇S₂Si₂

Guidance literature:: Multi-step reaction with 10 steps

1: PPTS / CH₂Cl₂

2: n-BuLi / tetrahydrofuran

3: Amberlyst-15E / methanol

4: Jones' reagent / acetone

5: I(collidine)2PF₆ / CH₂Cl₂

6: BF₃*OEt₂ / CH₂Cl₂

7: DIBAL-H / CH₂Cl₂

8: DBU / tetrahydrofuran

9: 69 percent / n-BuLi

With n-butyllithium; jones' reagent; Amberlyst-15E; boron trifluoride diethyl etherate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1016/S0040-4039(01)00286-6