2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine

Base Information

Chemical Name:2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine
CAS No.:1536349-41-3
Molecular Formula:C₂₉H₂₄Cl₂O₄S₂
Molecular Weight:571.545
Hs Code.:

Synonyms:2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine

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Chemical Property of 2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine

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Technology Process of 2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine

There total 1 articles about 2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1536349-10-6
6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine-2,10-diol

: 74-88-4
methyl iodide

: 1536349-41-3
2,10-dimethoxy-6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine

Guidance literature:: 6,6-dimethyl-3,9-bis((4-chlorophenyl)thio)dibenzo[d,f][1,3]dioxepine-2,10-diol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

methyl iodide; With 18-crown-6 ether; at 0 - 20 ℃; for 24.25h; Inert atmosphere;
DOI:10.1021/jo402522y