Technology Process of C35H64O5Si2
There total 14 articles about C35H64O5Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 100 percent / TEA; DMAP / CH2Cl2
2: 94 percent / AcOH; H2O / tetrahydrofuran / 50 °C
3: 98 percent / K2CO3 / methanol; CH2Cl2
4: 99 percent / MeI; NaHCO3 / H2O; acetone / 40 °C
5: 99 percent / H2; quinoline / Lindlar cat. / ethyl acetate
6: 65 percent / Eu(fod)3 / xylene / 120 °C
7: 99 percent / AgNO3; pyridine / acetonitrile
With
pyridine; quinoline; dmap; TEA; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; Eu(fod)3; methyl iodide;
Lindlar catalyst;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene;
DOI:10.1246/cl.2007.278
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / K2CO3 / methanol; CH2Cl2
2: 99 percent / MeI; NaHCO3 / H2O; acetone / 40 °C
3: 99 percent / H2; quinoline / Lindlar cat. / ethyl acetate
4: 65 percent / Eu(fod)3 / xylene / 120 °C
5: 99 percent / AgNO3; pyridine / acetonitrile
With
pyridine; quinoline; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; Eu(fod)3; methyl iodide;
Lindlar catalyst;
In
methanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene;
DOI:10.1246/cl.2007.278