2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

Base Information

Chemical Name:2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate
CAS No.:1146467-82-4
Molecular Formula:C₃₂H₃₀N₃O₈P
Molecular Weight:615.579
Hs Code.:

Synonyms:2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

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Technology Process of 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

There total 1 articles about 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-mannopyranose

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 1146467-83-5
2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-mannopyranosyl diphenyl phosphate

: 1146467-82-4
2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

Guidance literature:: With dmap; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/acs.joc.5b00139

Reference yield: 81.0%

: 61893-74-1
allyl 2,3,6-tri-O-benzyl-α-D-galactopyranoside

: 1146467-82-4
2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

: allyl 4-O-(2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-galactopyranoside

: C₅₀H₅₃N₃O₁₀

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 3h; Molecular sieve; Inert atmosphere;
DOI:10.1021/acs.joc.5b00139

Reference yield:

: 1146467-82-4
2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-mannopyranosyl diphenyl phosphate

: 55697-50-2
methyl 2,4,6-tri-O-benzyl-α-D-galactopyranoside

: 1146467-86-8
C₄₈H₅₁N₃O₁₀

: C₄₈H₅₁N₃O₁₀

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 4h; optical yield given as %de; diastereoselective reaction; Molecular sieve;
DOI:10.3987/COM-08-S(F)108