6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

Base Information

Chemical Name:6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal
CAS No.:1033614-52-6
Molecular Formula:C₂₀H₂₆O₉S
Molecular Weight:442.487
Hs Code.:

Synonyms:6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

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Technology Process of 6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

There total 1 articles about 6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033614-33-3
6-O-[6'-O-(benzyl)-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-3-O-(t-butyldimethylsilyl)-D-glucal

: 1033614-52-6
6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol800793f

Reference yield:

: 1033614-31-1
3-O-(t-butyldimethylsilyl)-4-O-mesyl-D-glucal

: 1033614-52-6
6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal

: 1033614-54-8
6-O-[6'-O-[6''-O-(benzyl)-2'',3''-dideoxy-β-D-threo-hex-2''-enopyranosyl]-2',3'-dideoxy-β-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-3-O-(t-butyldimethylsilyl)-D-glucal

Guidance literature:: 6-O-[6'-O-(benzyl)-2',3'-dideoxy-D-threo-hex-2'-enopyranosyl]-4-O-mesyl-D-glucal; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

3-O-(t-butyldimethylsilyl)-4-O-mesyl-D-glucal; In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol800793f