5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

Base Information

Chemical Name:5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane
CAS No.:185384-96-7
Molecular Formula:C₄₉H₆₈Cl₂O₆
Molecular Weight:823.981
Hs Code.:

Synonyms:5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

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Chemical Property of 5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

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Technology Process of 5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

There total 3 articles about 5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154023-65-1
3,3'-dichloro-4,4'-dimethoxy-5,5'-bis(methoxycarbonyl)benzophenone

: C₆₀H₁₀₄

: 185384-96-7
5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

Guidance literature:: With TiCl₃-1,2-dimethoxyethane; copper; zinc; In 1,2-dimethoxyethane; for 1h; Heating;
DOI:10.1016/0968-0896(96)00159-9

Reference yield:

: (5R,6S,8S,9S,10S,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-6-((E)-3-methoxy-allyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene

: 185384-96-7
5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / aq. HClO₄ / diethyl ether / 1.5 h / Ambient temperature

2: 39.5 mg / TiCl₃-DME, Zn-Cu, 3,3'-dicarbomethoxy-5,5'-dichloro-4,4'-dimethoxybenzophenone / 1,2-dimethoxy-ethane / 1 h / Heating

With perchloric acid; TiCl₃-1,2-dimethoxyethane; copper; 3,3'-dichloro-4,4'-dimethoxy-5,5'-bis(methoxycarbonyl)benzophenone; zinc; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/0968-0896(96)00159-9

Reference yield:

: 185384-94-5
(5α)-6β-(2'-formylethyl)cholestane

: C₆₀H₁₀₄

: 185384-96-7
5α-6β-[4',4'-(3'',3'''-dicarbomethoxy-5'',5'''-dichloro-4'',4'''-dimethoxydiphenyl)-3'-butenyl]cholestane

Guidance literature:: With TiCl₃-1,2-dimethoxyethane; copper; 3,3'-dichloro-4,4'-dimethoxy-5,5'-bis(methoxycarbonyl)benzophenone; zinc; In 1,2-dimethoxyethane; for 1h; Heating;
DOI:10.1016/0968-0896(96)00159-9