C₃₃H₅₀O₆Si

Base Information

Chemical Name:C₃₃H₅₀O₆Si
CAS No.:123358-18-9
Molecular Formula:C₃₃H₅₀O₆Si
Molecular Weight:570.842
Hs Code.:

C<sub>33</sub>H<sub>50</sub>O<sub>6</sub>Si

Synonyms:C₃₃H₅₀O₆Si

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Chemical Property of C₃₃H₅₀O₆Si

Chemical Property:

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Technology Process of C₃₃H₅₀O₆Si

There total 1 articles about C₃₃H₅₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 123357-94-8
C₃₃H₄₈O₆Si

: 123358-18-9
C₃₃H₅₀O₆Si

Guidance literature:: With hydrogen; RhCl(PPh₃)3; In benzene; under 760 Torr;
DOI:10.1021/ja00206a050

Reference yield:

: 123358-18-9
C₃₃H₅₀O₆Si

: C₃₄H₄₀O₈

Guidance literature:: Multi-step reaction with 13 steps

1: DIBAH / toluene / -78 °C

2: PCC / CH₂Cl₂

3: 1.) LDA, TMSCl / 1.) THF, 2.) CH₂Cl₂

4: 78 percent / benzene

5: 1.) m-CPBA, 2.) P(OEt)3 / 1.) CH₂Cl₂, 2.) C₆H₆, 60 deg C

6: tetrahydrofuran; CH₂Cl₂ / -78 °C

8: PCC / CH₂Cl₂

9: 92 percent / NaBH(OAc)3 / tetrahydrofuran / 60 °C

10: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH₂Cl₂

11: 50 percent / SeO₂, t-BuOOH / CH₂Cl₂ / 0 °C

12: 1.) SOCl₂, propylene oxide, 2.) KOBz, DMAP / 1.) Et₂O, 2.) CH₃CN

13: HClO₄, Montmorillonite clay (K₁₀) / methanol; ethane-1,2-diol

With tert.-butylhydroperoxide; dmap; chloro-trimethyl-silane; selenium(IV) oxide; thionyl chloride; perchloric acid; Montmorillonite clay (K₁₀); Potassium benzoate; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; methyloxirane; lithium diisopropyl amide; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; ethylene glycol; toluene; benzene;
DOI:10.1021/ja00206a050

Reference yield:

: 123358-18-9
C₃₃H₅₀O₆Si

: C₃₇H₄₄O₇

Guidance literature:: Multi-step reaction with 10 steps

1: DIBAH / toluene / -78 °C

2: PCC / CH₂Cl₂

3: 1.) LDA, TMSCl / 1.) THF, 2.) CH₂Cl₂

4: 78 percent / benzene

5: 1.) m-CPBA, 2.) P(OEt)3 / 1.) CH₂Cl₂, 2.) C₆H₆, 60 deg C

6: tetrahydrofuran; CH₂Cl₂ / -78 °C

8: PCC / CH₂Cl₂

9: 92 percent / NaBH(OAc)3 / tetrahydrofuran / 60 °C

10: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH₂Cl₂

With dmap; chloro-trimethyl-silane; sodium tris(acetoxy)borohydride; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide; triethyl phosphite; In tetrahydrofuran; dichloromethane; toluene; benzene;
DOI:10.1021/ja00206a050