L-3,3-diphenylalaninesultam hydrochloride

Base Information

Chemical Name:L-3,3-diphenylalaninesultam hydrochloride
CAS No.:138566-20-8
Molecular Formula:C₂₅H₃₀N₂O₃S*ClH
Molecular Weight:475.052
Hs Code.:

Synonyms:L-3,3-diphenylalaninesultam hydrochloride

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Chemical Property of L-3,3-diphenylalaninesultam hydrochloride

Chemical Property:

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Technology Process of L-3,3-diphenylalaninesultam hydrochloride

There total 4 articles about L-3,3-diphenylalaninesultam hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 138566-19-5
N-(diphenylmethylene)-L-3,3-diphenylalaninesultam

: 119-61-9
benzophenone

: 138566-20-8
L-3,3-diphenylalaninesultam hydrochloride

Guidance literature:: With hydrogenchloride; silica gel; In chloroform; at 40 ℃; for 2h; sonication;
DOI:10.1016/0040-4039(91)80217-T

Reference yield: 89.0%

: 138566-19-5
N-(diphenylmethylene)-L-3,3-diphenylalaninesultam

: 138566-20-8
L-3,3-diphenylalaninesultam hydrochloride

Guidance literature:: With hydrogenchloride; silica gel; In chloroform; at 40 ℃; for 2h;
DOI:10.1021/jm00037a009

Reference yield:

: 138566-17-3
2-(benzhydrylideneamino)-1-(10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1.5]dec-4-yl)ethanone

: 138566-20-8
L-3,3-diphenylalaninesultam hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, HMPA / 1.) hexane, THF, from -78 deg C to RT, 2.) hexane, THF, RT, 5 d

2: 89 percent / 0.5 N aq. HCl, silica gel / CHCl₃ / 2 h / 40 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; silica gel; In chloroform;
DOI:10.1021/jm00037a009