pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside
CAS No.:263758-95-8
Molecular Formula:C₂₆H₂₅Cl₄NO₇
Molecular Weight:605.299
Hs Code.:

Synonyms:pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

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Chemical Property of pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

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Technology Process of pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

There total 2 articles about pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 174356-32-2
pent-4-enyl 4,6-O-benzylidene-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

: 263758-95-8
pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h;
DOI:10.1080/07328300008544063

Reference yield: 69.0%

: 100-39-0
benzyl bromide

: 182002-91-1
pent-4-enyl 2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

: 263758-95-8
pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

Guidance literature:: pent-4-enyl 2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside; With bis(tri-n-butyltin)oxide; In methanol; at 75 ℃; for 2h;

benzyl bromide; With tetrabutylammomium bromide; at 90 ℃; for 20h;
DOI:10.1081/CAR-100108275

Reference yield: 87.0%

: 290330-34-6
2,3,4-tri-O-acetyl-6-O-benzyl-α-D-galactopyranosyl bromide

: 263758-95-8
pent-4-enyl 6-O-benzyl-2-tetrachlorophthalimido-2-deoxy-β-D-glucopyranoside

: 403832-86-0
pent-4-enyl (2,3,4-tri-O-acetyl-6-O-benzyl-β-D-galactopyranosyl)-(1->4)-6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

Guidance literature:: With 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -60 ℃; for 1h;
DOI:10.1081/CAR-100108275