4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

Base Information

Chemical Name:4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride
CAS No.:1331775-18-8
Molecular Formula:C₂₈H₃₅N₃O₂*ClH
Molecular Weight:482.066
Hs Code.:

Synonyms:4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

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Chemical Property of 4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

Chemical Property:

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Technology Process of 4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

There total 6 articles about 4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1331773-95-5
4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy)pyridazine

: 1331775-18-8
4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane;

Reference yield:

: 1331775-09-7
1-(4-benzyloxyphenyl)hexan-2-one

: 1331775-18-8
4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / toluene / 16 h / 20 °C

2.1: hydrazine hydrate / acetic acid / 4 h / 120 °C

3.1: trichlorophosphate / 2 h / 70 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

4.2: 50 - 55 °C

5.1: hydrogenchloride / 1,4-dioxane / 0.75 h / 20 °C

6.1: dichloromethane / 20 °C

7.1: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; sodium hydride; hydrazine hydrate; triethylamine; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetic acid; toluene; mineral oil;

Reference yield:

: 1331775-10-0
3-(4-benzyloxyphenyl)-2-hydroxy-4-oxooctanoic acid ethyl ester

: 1331775-18-8
4-(4-benzyloxyphenyl)-3-butyl-6-(1-methylpiperidin-4-ylmethoxy) pyridazine hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrazine hydrate / acetic acid / 4 h / 120 °C

2.1: trichlorophosphate / 2 h / 70 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

3.2: 50 - 55 °C

4.1: hydrogenchloride / 1,4-dioxane / 0.75 h / 20 °C

5.1: dichloromethane / 20 °C

6.1: hydrogenchloride / 1,4-dioxane

With hydrogenchloride; sodium hydride; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetic acid; mineral oil;