Technology Process of C26H27N3O6
There total 7 articles about C26H27N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 48h;
DOI:10.1016/j.bmc.2010.06.081
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tris-(o-tolyl)phosphine / palladium diacetate / N,N-dimethyl-formamide / 24 h / 130 °C / Inert atmosphere
2.1: sodium tetrahydroborate / ethanol / 20 °C
3.1: triethylamine / tetrahydrofuran / 1 h / 0 °C
4.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C
4.2: 20 °C
5.1: hydrogenchloride / hexanes; diethyl ether / 20 °C
6.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C
With
4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; tris-(o-tolyl)phosphine;
palladium diacetate;
In
tetrahydrofuran; hexanes; diethyl ether; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tris-(o-tolyl)phosphine / palladium diacetate / N,N-dimethyl-formamide / 24 h / 130 °C / Inert atmosphere
2.1: sodium tetrahydroborate / ethanol / 20 °C
3.1: triethylamine / tetrahydrofuran / 1 h / 0 °C
4.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C
4.2: 20 °C
5.1: hydrogenchloride / hexanes; diethyl ether / 20 °C
6.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C
With
4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; tris-(o-tolyl)phosphine;
palladium diacetate;
In
tetrahydrofuran; hexanes; diethyl ether; ethanol; N,N-dimethyl-formamide;