phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid

Base Information

Chemical Name:phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid
CAS No.:1242584-18-4
Molecular Formula:C₂₄H₂₅N₂O₅P
Molecular Weight:452.447
Hs Code.:

Synonyms:phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid

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Chemical Property of phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid

Chemical Property:

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Technology Process of phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid

There total 2 articles about phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-50-7
ethyl 2-hydroxyacetate

: 886-64-6
N^β-benzyloxycarbonyl-β-alaninamide

: 100-52-7
benzaldehyde

: 644-97-3
Dichlorophenylphosphine

: 1242584-18-4
phenyl[N-(R,S)-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinic acid

: ethyl [[phenyl[N-[N-benzyloxycarbonyl-β-alaninyl]-1-aminophenylmethyl]phosphinyl]oxy]acetate

: C₂₈H₃₁N₂O₇P

Guidance literature:: N^β-benzyloxycarbonyl-β-alaninamide; benzaldehyde; Dichlorophenylphosphine; In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

ethyl 2-hydroxyacetate; With triethylamine; In acetonitrile; at 20 ℃; for 6h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.032