(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

Base Information

Chemical Name:(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt
CAS No.:1460202-47-4
Molecular Formula:C₈H₁₁N*C₁₅H₁₄O₅
Molecular Weight:395.455
Hs Code.:

Synonyms:(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

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Chemical Property of (S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

Chemical Property:

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Technology Process of (S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

There total 5 articles about (S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1460202-45-2
3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid

: 1460202-47-4
(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

Guidance literature:: In isopropyl alcohol; at 20 - 65 ℃;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1460202-47-4
(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / 40 h / 115 - 120 °C

2.1: lithium hydroxide; water / N,N-dimethyl-formamide / 60 - 70 °C

3.1: methanol; palladium on activated charcoal; hydrogen / N,N-dimethyl-formamide / 60 - 65 °C / 6000.6 - 7500.75 Torr

3.2: 20 °C

4.1: isopropyl alcohol / 20 - 65 °C

With methanol; palladium on activated charcoal; water; hydrogen; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1460202-47-4
(S)-3-(2,4-dihydroxyphenyl)-2-(4-hydroxyphenyl)propanoic acid (S)-α-methylbenzylamine salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / 40 h / 115 - 120 °C

2.1: lithium hydroxide; water / N,N-dimethyl-formamide / 60 - 70 °C

3.1: methanol; palladium on activated charcoal; hydrogen / N,N-dimethyl-formamide / 60 - 65 °C / 6000.6 - 7500.75 Torr

3.2: 20 °C

4.1: isopropyl alcohol / 20 - 65 °C

With methanol; palladium on activated charcoal; water; hydrogen; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In N,N-dimethyl-formamide; isopropyl alcohol;