C₃₆H₆₆O₉SSi₂

Base Information

Chemical Name:C₃₆H₆₆O₉SSi₂
CAS No.:934618-04-9
Molecular Formula:C₃₆H₆₆O₉SSi₂
Molecular Weight:731.152
Hs Code.:

C<sub>36</sub>H<sub>66</sub>O<sub>9</sub>SSi<sub>2</sub>

Synonyms:C₃₆H₆₆O₉SSi₂

Suppliers and Price of C₃₆H₆₆O₉SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₆₆O₉SSi₂

Chemical Property:

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Technology Process of C₃₆H₆₆O₉SSi₂

There total 18 articles about C₃₆H₆₆O₉SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 934618-03-8
C₃₅H₆₄O₇Si₂

: 124-63-0
methanesulfonyl chloride

: 934618-04-9
C₃₆H₆₆O₉SSi₂

Guidance literature:: With dmap; TEA; In dichloromethane;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-86-4
C₃₇H₆₈O₆SSi₂

: 934618-04-9
C₃₆H₆₆O₉SSi₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 100 percent / TEA; DMAP / CH₂Cl₂

2.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

3.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

4.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

5.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

6.1: 65 percent / Eu(fod)3 / xylene / 120 °C

7.1: 99 percent / AgNO₃; pyridine / acetonitrile

8.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

9.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

11.1: 97 percent / DMAP; TEA / CH₂Cl₂

With pyridine; quinoline; dmap; sodium tetrahydroborate; TEA; diphenyl diselenide; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-99-9
C₃₂H₅₆O₈S₂Si

: 934618-04-9
C₃₆H₆₆O₉SSi₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

2.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

3.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

4.1: 65 percent / Eu(fod)3 / xylene / 120 °C

5.1: 99 percent / AgNO₃; pyridine / acetonitrile

6.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

7.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

7.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

8.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

9.1: 97 percent / DMAP; TEA / CH₂Cl₂

With pyridine; quinoline; dmap; sodium tetrahydroborate; TEA; diphenyl diselenide; hydrogen; sodium hydrogencarbonate; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278