N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

Base Information

Chemical Name:N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide
CAS No.:439926-95-1
Molecular Formula:C₂₆H₂₈N₄O₄S
Molecular Weight:492.599
Hs Code.:

Synonyms:N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

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Technology Process of N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

There total 7 articles about N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 439926-95-1
N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

Guidance literature:

Reference yield:

: 24964-64-5
3-Cyanobenzaldehyde

: 439926-95-1
N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / Heating

2.1: H₂ / Pd/C / methanol

3.1: CH₂Cl₂

3.2: DIEA / CH₂Cl₂

4.1: HCl (gas); AcOH

5.1: Et₃N / CH₂Cl₂

With hydrogenchloride; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2003.12.083

Reference yield:

: 386768-80-5
N'-[1-(3-Cyano-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid tert-butyl ester

: 439926-95-1
N'-(1-Azepanylcarbonyl)-N'-(3-cyanobenzyl)-6-methoxy-2-naphthalenesulfonohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: H₂ / Pd/C / methanol

2.1: CH₂Cl₂

2.2: DIEA / CH₂Cl₂

3.1: HCl (gas); AcOH

4.1: Et₃N / CH₂Cl₂

With hydrogenchloride; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2003.12.083