(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

Base Information

Chemical Name:(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate
CAS No.:1580522-29-7
Molecular Formula:C₂₁H₂₃NO₆S
Molecular Weight:417.483
Hs Code.:

Synonyms:(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

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Chemical Property of (R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

Chemical Property:

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Technology Process of (R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

There total 3 articles about (R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353021-67-6
(R)-6-hydroxy-1-phenylhex-1-yn-3-yl methyl carbonate

: 1580522-29-7
(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 70 °C / Inert atmosphere

3: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: 55125-01-4
N-(t-butoxycarboyl)-4-methoxyphenylsulfonamide

: 1580522-29-7
(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 70 °C / Inert atmosphere

3: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: C₂₆H₃₁NO₈S

: 1580522-29-7
(R)-6-(4-methoxyphenylsulfonamido)-1-phenylhex-1-yn-3-yl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 70 °C / Inert atmosphere

2: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; potassium carbonate; In methanol; dichloromethane;
DOI:10.1002/anie.201309162