6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

Base Information

Chemical Name:6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid
CAS No.:407602-76-0
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

Synonyms:6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

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Chemical Property of 6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

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Technology Process of 6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

There total 2 articles about 6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17811-33-5
5-(3',3'-dimethylallyloxy)-7-methoxy-6-methylphthalide

: 407602-76-0
6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

Guidance literature:: With methanol; potassium carbonate; at 24 ℃; Heating;
DOI:10.1021/jf010641t

Reference yield:

: 17811-28-8
zinniol

: 407602-76-0
6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / CrO₃; H₂SO₄ / acetone; H₂O / 0.08 h / 20 °C

2: K₂CO₃; MeOH / 24 °C / Heating

With chromium(VI) oxide; methanol; sulfuric acid; potassium carbonate; In water; acetone; 1: Jones oxidation;
DOI:10.1021/jf010641t

Reference yield: 57.0%

: 407602-76-0
6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid

: 74-88-4
methyl iodide

: methyl-2-methoxy-3-methyl-4-(3',3'-dimethylallyloxy)-6-methoxymethyl benzoate

: 2-methoxy-3-methyl-4-(3',3'-dimethylallyloxy)-6-methoxymethyl benzoic acid

Guidance literature:: 6-hydroxymethyl-2-methoxy-3-methyl-4-(3-methyl-but-2-enyloxy)-benzoic acid; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 44h;
DOI:10.1021/jf010641t