pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

Base Information

Chemical Name:pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester
CAS No.:1369590-69-1
Molecular Formula:C₁₉H₂₇N₃O₄
Molecular Weight:361.441
Hs Code.:

Synonyms:pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

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Chemical Property of pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

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Technology Process of pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

There total 5 articles about pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-98-1
2-Hydroxymethylpyridine

: 1369590-91-9
pyrrolidine-1-carboxylic acid 4-amino-cyclohexylmethyl ester

: 530-62-1
1,1'-carbonyldiimidazole

: 1369590-69-1
pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

Guidance literature:: 2-Hydroxymethylpyridine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h;

pyrrolidine-1-carboxylic acid 4-amino-cyclohexylmethyl ester; In tetrahydrofuran; at 60 ℃; for 2h;

Reference yield:

: 1369590-89-5
pyrrolidine-1-carboxylic acid 4-hydroxy-cyclohexylmethyl ester

: 1369590-69-1
pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Oxone; tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 14 h

2.1: hydroxylamine / ethanol / 5 h / Reflux

3.1: hydrogen; ammonia / Raney nickel / methanol / 12 h

4.1: tetrahydrofuran / 2 h / 20 °C

4.2: 2 h / 60 °C

With Oxone; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; ammonia; hydrogen; hydroxylamine; Raney nickel; In tetrahydrofuran; methanol; ethanol; dichloromethane;

Reference yield:

: 1369590-90-8
pyrrolidine-1-carboxylic acid 4-oxo-cyclohexylmethyl ester

: 1369590-69-1
pyrrolidine-1-carboxylic acid 4-(pyridin-2-ylmethoxycarbonylamino)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine / ethanol / 5 h / Reflux

2.1: hydrogen; ammonia / Raney nickel / methanol / 12 h

3.1: tetrahydrofuran / 2 h / 20 °C

3.2: 2 h / 60 °C

With ammonia; hydrogen; hydroxylamine; Raney nickel; In tetrahydrofuran; methanol; ethanol;