[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

Base Information

Chemical Name:[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine
CAS No.:144543-12-4
Molecular Formula:C₂₄H₂₈N₂OSi
Molecular Weight:388.585
Hs Code.:

Synonyms:[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

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Chemical Property of [(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

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Technology Process of [(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

There total 6 articles about [(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid (E)-4-(tert-butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl ester

: 144543-12-4
[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

Guidance literature:: With triethylamine; hydrazine; In tetrahydrofuran; methanol; at 0 ℃; for 12h;

Reference yield:

: 124044-22-0
(1,1-dimethylethyl)<(2-bromo-2-pentene-5-trimethylsilyl-4-ynyl)oxy>diphenylsilane

: 144543-12-4
[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / CuI, bis(triphenylphosphine)palladium(II) chloride, n-propylamine / tetrahydrofuran / 14 h / 23 °C

2: 95 percent / aq. NaOH / methanol / 45 h / 0 °C

3: triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

4: anhydr. hydrazine, triethylamine / tetrahydrofuran; methanol / 12 h / 0 °C

With propylamine; sodium hydroxide; copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 124044-21-9
(Z)-2-Bromo-5-trimethylsilanyl-pent-2-en-4-ynoic acid ethyl ester

: 144543-12-4
[(E)-4-(tert-Butyl-diphenyl-silanyloxymethyl)-hept-4-ene-2,6-diynyl]-hydrazine

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / diisobutylaluminum hydride / hexane; toluene / a) -78 deg C, 30 min, b) 0 deg C, 30 min

2: 95 percent / 4-(dimethylamino)pyridine, triethylamine / tetrahydrofuran / 3.5 h / 23 °C

3: 86 percent / CuI, bis(triphenylphosphine)palladium(II) chloride, n-propylamine / tetrahydrofuran / 14 h / 23 °C

4: 95 percent / aq. NaOH / methanol / 45 h / 0 °C

5: triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

6: anhydr. hydrazine, triethylamine / tetrahydrofuran; methanol / 12 h / 0 °C

With propylamine; dmap; sodium hydroxide; copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; diisobutylaluminium hydride; triethylamine; hydrazine; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene;