K{Co(2,6-Me₂C₆H₃NC)4}

Base Information

Chemical Name:K{Co(2,6-Me₂C₆H₃NC)4}
CAS No.:121255-01-4
Molecular Formula:C₃₆H₃₆CoN₄*K
Molecular Weight:622.8
Hs Code.:

K{Co(2,6-Me<sub>2</sub>C<sub>6</sub>H<sub>3</sub>NC)4}

Synonyms:K{Co(2,6-Me₂C₆H₃NC)4}

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Chemical Property of K{Co(2,6-Me₂C₆H₃NC)4}

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Technology Process of K{Co(2,6-Me₂C₆H₃NC)4}

There total 6 articles about K{Co(2,6-Me₂C₆H₃NC)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: potassium naphthalenide

: 64707-28-4
Co2<2,6-Me2C6H3NC>8

: 121255-01-4
K{Co(2,6-Me₂C₆H₃NC)4}

Guidance literature:: In tetrahydrofuran; under N2; soln. Co-complex/THF cooled to -78°C, dropwise addn. soln. of K(C10H8)/THF, soln. changed from orange-red to deep blood-red, soln. allowed to warm (15 min); concd. (vac.), carefully layered with hexane, layers allowed to mix slowly by diffusion at -80°C until the soln. appeared uniform, elem.anal.;
DOI:10.1021/ja00098a017

Reference yield: 73.0%

: 121232-42-6
K⁽¹⁺⁾*{Co(C₂H₄)4}^(1-)=K{Co(C₂H₄)4}

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 121255-01-4
K{Co(2,6-Me₂C₆H₃NC)4}

Guidance literature:: In tetrahydrofuran; at room temp.; effervescence; deep orange-red soln. after 5 min; concn. under reduced pressure; stirring; addn. of pentane; pptn.; elem. anal.;

Reference yield:

: 121232-43-7
[Co(2,6-dimethylphenyl isocyanide)4]^(1-)

: 121255-01-4
K{Co(2,6-Me₂C₆H₃NC)4}

Guidance literature:: Multi-step reaction with 2 steps

1: H⁽¹⁺⁾ / not given

2: tetrahydrofuran

With H⁽¹⁺⁾; In tetrahydrofuran;
DOI:10.1021/ja00098a017